The ball mill method made the metal oxide particles distributed evenly on GNS with the shape more regular and the size smaller. Figure 2 (c) shows the CuO-ZnO-Al 2 O 3 catalysts doped with 10 wt.% GNS with the smallest size distributed on the GNS sheets most uniformly which is consistent with the change of the grain size of CuO and ZnO.
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DetailsSynth). A planetary ball mill (Fritsch, Pulverissette 6 Mono-Mill) was used with stainless steel balls having diam eters of 5, 10, and 20 mm. The milling was conducted at room temperature, maintaining a constant speed of 500 rpm for 1 h, pausing every 10 min to remove the material from the jar wall and to avoid overheating. No water was added ...
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DetailsSamples were milled in a laboratory ball mill to the desired fineness. Particle size distribution curves, including d 50 and d 90, were determined using laser granulometry (Mastersizer 2000 from Malvern Instruments). The mineral phases present in each sample were investigated using XRD.
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DetailsAfter calcination, both clays were ground in a Servitech planetary ball mill for 3 min, model CT-242, in porcelain jars with a capacity of 1000 mL and rotation of 380 rpm with a proportion in volume of 1/3 of the material for 2/3 of ceramic balls with 5 mm diameter. The characterization of the materials is presented in Table 1.
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Detailslaboratory ball mill for at least 3 hours, using polymer balls to prevent further grinding of the materials. Paste samples were prepared at 0.5 w/b ratio, and mixing performed on a vortex mixer for 2 minutes. Isothermal conduction calorimetry, thermogravimetric analysis (TGA)
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